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Versailles project on advanced materials and standards (VAMAS) interlaboratory study on measuring the number concentration of colloidal gold nanoparticles

Minelli, Caterina and Wywijas, Magdalena and Bartczak, Dorota and Wywijas, Magdalena and Cuello-Nunez, Susana and Infante, Heidi Goenaga and Deumer, Jerome and Gollwitzer, Christian and Krumrey, Michael and Murphy, Karen E. and Johnson, Monique E. and Bustos, Antonio R. Montoro and Strenge, Ingo H. and Faure, Bertrand and Hoghoj, Peter and Tong, Vivian and Burr, Loic and Norling, Karin and Hook, Fredrik and Roesslein, Matthias and Kocic, Jovana and Hendriks, Lyndsey and Kestens, Vikram and Ramaye, Yannic and Lopez, Maria C. Contreras and Auclair, Guy and Mehn, Dora and Gilliland, Douglas and Potthoff, Annegret and Oelschlagel, Kathrin and Tentschert, Jutta and Jungnickel, Harald and Krause, Benjamin C. and Hachenberger, Yves U. and Reichardt, Philipp and Luch, Andreas and Whittaker, Thomas E. and Stevens, Molly M. and Gupta, Shalini and Singh, Akash and Lin, Fang-hsin and Liu, Yi-Hung and Costa, Anna Luisa and Baldisserri, Carlo and Jawad, Rid and Andaloussi, Samir E. L. and Holme, Margaret N. and Lee, Tae Geol and Kwak, Minjeong and Kim, Jaeseok and Ziebel, Johanna and Guignard, Cedric and Cambier, Sebastien and Contal, Servane and Gutleb, Arno C. and Tatarkiewicz, Jan Kuba and Jankiewicz, Bartlomiej J. and Bartosewicz, Bartosz and Wu, Xiaochun and Fagan, Jeffrey A. and Elje, Elisabeth and Runden-Pran, Elise and Dusinska, Maria and Kaur, Inder Preet and Price, David and Nesbitt, Ian and O'Reilly, Sarah and Peters, Ruud J. B. and Bucher, Guillaume and Coleman, Dennis and Harrison, Angela J. and Ghanem, Antoine and Gering, Anne and McCarron, Eileen and Fitzgerald, Niamh and Cornelis, Geert and Tuoriniemi, Jani and Sakai, Midori and Tsuchida, Hidehisa and Maguire, Ciaran and Prina-Mello, Adriele and Lawlor, Alan J. and Adams, Jessica and Schultz, Carolin L. and Constantin, Doru and Thanh, Nguyen Thi Kim and Tung, Le Duc and Panariello, Luca and Damilos, Spyridon and Gavriilidis, Asterios and Lynch, Iseult and Fryer, Benjamin and Quevedo, Ana Carrazco and Guggenheim, Emily and Briffa, Sophie and Valsami-Jones, Eugenia and Huang, Yuxiong and Keller, Arturo A. and Kinnunen, Virva-Tuuli and Peramaki, Siiri and Krpetic, Zeljka and Greenwood, Michael and Shard, Alexander G. (2022). Versailles project on advanced materials and standards (VAMAS) interlaboratory study on measuring the number concentration of colloidal gold nanoparticles. Nanoscale. 14 :12 , 4690-4704
[Research article]

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Abstract

We describe the outcome of a large international interlaboratory study of the measurement of particle number concentration of colloidal nanoparticles, project 10 of the technical working area 34, "Nanoparticle Populations" of the Versailles Project on Advanced Materials and Standards (VAMAS). A total of 50 laboratories delivered results for the number concentration of 30 nm gold colloidal nanoparticles measured using particle tracking analysis (PTA), single particle inductively coupled plasma mass spectrometry (spICP-MS), ultraviolet-visible (UV-Vis) light spectroscopy, centrifugal liquid sedimentation (CLS) and small angle X-ray scattering (SAXS). The study provides quantitative data to evaluate the repeatability of these methods and their reproducibility in the measurement of number concentration of model nanoparticle systems following a common measurement protocol. We find that the population-averaging methods of SAXS, CLS and UV-Vis have high measurement repeatability and reproducibility, with between-labs variability of 2.6%, 11% and 1.4% respectively. However, results may be significantly biased for reasons including inaccurate material properties whose values are used to compute the number concentration. Particle-counting method results are less reproducibile than population-averaging methods, with measured between-labs variability of 68% and 46% for PTA and spICP-MS respectively. This study provides the stakeholder community with important comparative data to underpin measurement reproducibility and method validation for number concentration of nanoparticles.

Authors/Creators:Minelli, Caterina and Wywijas, Magdalena and Bartczak, Dorota and Wywijas, Magdalena and Cuello-Nunez, Susana and Infante, Heidi Goenaga and Deumer, Jerome and Gollwitzer, Christian and Krumrey, Michael and Murphy, Karen E. and Johnson, Monique E. and Bustos, Antonio R. Montoro and Strenge, Ingo H. and Faure, Bertrand and Hoghoj, Peter and Tong, Vivian and Burr, Loic and Norling, Karin and Hook, Fredrik and Roesslein, Matthias and Kocic, Jovana and Hendriks, Lyndsey and Kestens, Vikram and Ramaye, Yannic and Lopez, Maria C. Contreras and Auclair, Guy and Mehn, Dora and Gilliland, Douglas and Potthoff, Annegret and Oelschlagel, Kathrin and Tentschert, Jutta and Jungnickel, Harald and Krause, Benjamin C. and Hachenberger, Yves U. and Reichardt, Philipp and Luch, Andreas and Whittaker, Thomas E. and Stevens, Molly M. and Gupta, Shalini and Singh, Akash and Lin, Fang-hsin and Liu, Yi-Hung and Costa, Anna Luisa and Baldisserri, Carlo and Jawad, Rid and Andaloussi, Samir E. L. and Holme, Margaret N. and Lee, Tae Geol and Kwak, Minjeong and Kim, Jaeseok and Ziebel, Johanna and Guignard, Cedric and Cambier, Sebastien and Contal, Servane and Gutleb, Arno C. and Tatarkiewicz, Jan Kuba and Jankiewicz, Bartlomiej J. and Bartosewicz, Bartosz and Wu, Xiaochun and Fagan, Jeffrey A. and Elje, Elisabeth and Runden-Pran, Elise and Dusinska, Maria and Kaur, Inder Preet and Price, David and Nesbitt, Ian and O'Reilly, Sarah and Peters, Ruud J. B. and Bucher, Guillaume and Coleman, Dennis and Harrison, Angela J. and Ghanem, Antoine and Gering, Anne and McCarron, Eileen and Fitzgerald, Niamh and Cornelis, Geert and Tuoriniemi, Jani and Sakai, Midori and Tsuchida, Hidehisa and Maguire, Ciaran and Prina-Mello, Adriele and Lawlor, Alan J. and Adams, Jessica and Schultz, Carolin L. and Constantin, Doru and Thanh, Nguyen Thi Kim and Tung, Le Duc and Panariello, Luca and Damilos, Spyridon and Gavriilidis, Asterios and Lynch, Iseult and Fryer, Benjamin and Quevedo, Ana Carrazco and Guggenheim, Emily and Briffa, Sophie and Valsami-Jones, Eugenia and Huang, Yuxiong and Keller, Arturo A. and Kinnunen, Virva-Tuuli and Peramaki, Siiri and Krpetic, Zeljka and Greenwood, Michael and Shard, Alexander G.
Title:Versailles project on advanced materials and standards (VAMAS) interlaboratory study on measuring the number concentration of colloidal gold nanoparticles
Series Name/Journal:Nanoscale
Year of publishing :2022
Volume:14
Number:12
Page range:4690-4704
Number of Pages:15
Publisher:ROYAL SOC CHEMISTRY
ISSN:2040-3364
Language:English
Publication Type:Research article
Article category:Scientific peer reviewed
Version:Published version
Copyright:Creative Commons: Attribution-Noncommercial 3.0
Full Text Status:Public
Subjects:(A) Swedish standard research categories 2011 > 2 Engineering and Technology > 210 Nano Technology > Nano Technology
URN:NBN:urn:nbn:se:slu:epsilon-p-116589
Permanent URL:
http://urn.kb.se/resolve?urn=urn:nbn:se:slu:epsilon-p-116589
Additional ID:
Type of IDID
DOI10.1039/d1nr07775a
Web of Science (WoS)000766284600001
ID Code:27667
Faculty:NJ - Fakulteten för naturresurser och jordbruksvetenskap
Department:(NL, NJ) > Dept. of Soil and Environment
(S) > Dept. of Soil and Environment
Deposited By: SLUpub Connector
Deposited On:29 Apr 2022 14:45
Metadata Last Modified:29 Apr 2022 14:51

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